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Procedure for the Screening of Eggs and Egg Products to Detect Oxolonic Acid, Ciprofloxacin, Enrofloxacin, and Sarafloxacin Using Micellar Liquid Chromatography

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Procedure for the Screening of Eggs and Egg Products to Detect Oxolonic Acid, Ciprofloxacin, Enrofloxacin, and Sarafloxacin Using Micellar Liquid Chromatography

dc.contributor.author	Peris Vicente, Juan
dc.contributor.author	García-Ferrer, Daniel
dc.contributor.author	Mishra, Pooja
dc.contributor.author	Albiol-Chiva, Jaume
dc.contributor.author	Esteve i Romero, Josep-Salvador
dc.contributor.author	Carda Broch, Samuel
dc.date.accessioned	2023-11-20T14:40:58Z
dc.date.available	2023-11-20T14:40:58Z
dc.date.issued	2019
dc.identifier.uri	https://hdl.handle.net/10550/91261
dc.description.abstract	A method based on micellar liquid chromatography was developed to determine oxolinic acid, ciprofloxacin, enrofloxacin, and sarafloxacin in eggs and egg products. The antimicrobial drugs were obtained in a micellar solution which was directly injected. The analytes were resolved using a C18 column and a mobile phase of 0.05 M sodium dodecyl sulfate¿7.5% 1-propanol¿0.5% triethylamine, buffered at pH 3 with phosphate salt, running under the isocratic mode. The signal was monitored by fluorescence. Validation was successfully performed according to the EU Commission Decision 2002/657/EC in terms of specificity, calibration range (LOQ to 1 mg/kg), linearity (R2 > 0.9991), limit of detection and decision limit (0.01-0.05 mg/kg), limit of quantification (0.025-0.150 mg/kg), detection capability (<0.4 times decision limit), trueness (−14.2% to +9.8%), precision (<14.0%), robustness, and stability. The procedure was environmentally friendly, safe, easy-to-conduct, inexpensive, and had a high sample throughput, thus it is useful for routine analysis as a screening method in a laboratory for food residue control.
dc.language.iso	eng
dc.relation.ispartof	Antibiotics-Basel, 2019, vol. 8, num. 4, p. 226
dc.source	Peris Vicente, Juan, García-Ferrer, Daniel, Mishra, Pooja, Albiol-Chiva, Jaume, Esteve i Romero, Josep-Salvador, Carda Broch, Samuel (2019). Procedure for the Screening of Eggs and Egg Products to Detect Oxolonic Acid, Ciprofloxacin, Enrofloxacin, and Sarafloxacin Using Micellar Liquid Chromatography. Antibiotics-Basel, 8 4 226. https://doi.org/10.3390/antibiotics8040226
dc.subject	química analítica
dc.subject	residus
dc.subject	farmacologia
dc.title	Procedure for the Screening of Eggs and Egg Products to Detect Oxolonic Acid, Ciprofloxacin, Enrofloxacin, and Sarafloxacin Using Micellar Liquid Chromatography
dc.type	journal article
dc.date.updated	2023-11-20T14:40:58Z
dc.identifier.doi	10.3390/antibiotics8040226
dc.identifier.idgrec	135229
dc.rights.accessRights	open access